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At this point the colour change of the liquid had gone from a yellow, to a darker yellow, to an orange then all the way to a dark ruby red. The colour also seems to be a good indicator of when all of the 3,4,5 — TMBA has reacted, in these conditions look out for a dark blood ruby red but not blackish colour. 12) Once removed from heat, stirring stopped, crystals grow fairly quickly and within an hour...